U.S. flag

An official website of the United States government, Department of Justice.

NCJRS Virtual Library

The Virtual Library houses over 235,000 criminal justice resources, including all known OJP works.
Click here to search the NCJRS Virtual Library

Ballpoint Ink Age Determination by Volatile Component Comparison - A Preliminary Study

NCJ Number
98836
Journal
Journal of Forensic Sciences Volume: 30 Issue: 2 Dated: (April 1985) Pages: 405-411
Author(s)
L F Stewart
Date Published
1985
Length
7 pages
Annotation
Ballpoint pen inks consist primarily of a mixture of dyes, resins, and vehicle components.
Abstract
The vehicles are used to solubilize or suspend dyes, resins, and other components as well as to provide smooth ball morement and flow of ink onto writing surfaces. These vehicles are relatively volatile and make up approximately 50% of the ink by weight. Extraction and formulation identification of the questioned ink is performed. Once identified, the volatile components of the ink are measured quantitatively by gas chromatography. Preliminary studies show that the relative proportions of these volatile ingredients decrease as the ink ages. How long an ink has been on paper is determined by comparison of the relative concentrations of the volatile components of the questioned ink with those of known inks (age) of the same formulation. The relationship between age of ink, storage conditions, and paper will also be discussed. (Author abstract)